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1 article(s) from De Poli, Matteo

Partial thioamide scan on the lipopeptaibiotic trichogin GA IV. Effects on folding and bioactivity

Marta De Zotti,
Barbara Biondi,
Cristina Peggion,
Matteo De Poli,
Haleh Fathi,
Simona Oancea,
Claudio Toniolo and
Fernando Formaggio

Beilstein J. Org. Chem. 2012, 8, 1161–1171, doi:10.3762/bjoc.8.129

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Figure 1: List of primary structures and abbreviations for the peptides studied in this work. The [Leu¹¹-OMe]...

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Scheme 1: Synthesis of ψ[CS-NH]². 1: Coupling in the presence of EDC/HOBt. 2: Deprotection by using TFA/DCM. ...

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Scheme 2: Synthesis of ψ[CS-NH]⁵. 1: Coupling in the presence of EDC/HOBt. 2: Deprotection by using TFA/DCM. ...

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Scheme 3: Synthesis of ψ[CS-NH]⁹. 1: Deprotection by catalytic hydrogenation with Pd/C. 2: Coupling with n-Oc...

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Figure 2: RP-HPLC profiles obtained for [Leu¹¹-OMe] trichogin GA IV (tric-OMe) and its ψ[CS-NH]², ψ[CS-NH]⁵, ...

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Figure 3: Far-UV (panel I) and near-UV (panel II) CD spectra of [Leu¹¹-OMe] trichogin GA IV (tric-OMe) and it...

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Figure 4: FT-IR absorption spectra (3550–3200 cm⁻¹ region) in CDCl₃ solution of [Leu¹¹-OMe] trichogin GA IV (...

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Figure 5: Region of the amide NH protons in the H/H-ROESY spectrum of ψ[CS-NH]⁹ (400 MHz, 1 mM in CD₃CN solut...

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Figure 6: Fingerprint region of the H/H-ROESY spectrum of ψ[CS-NH]⁹ (400 MHz, 1 mM in CD₃CN solution, 298 K)....

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Figure 7: Fingerprint region of the H/H-ROESY spectrum of ψ[CS-NH]⁹ (400 MHz, 1 mM in CD₃CN solution, 298 K)....

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Figure 8: Ribbon representation of the lowest energy (138.7 kcal/mol) 3D structure obtained for ψ[CS-NH]⁹. Al...

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Published 24 Jul 2012

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